Chromatographic Methods in Clinical Chemistry and Toxicology

Implementation of liquid chromatography/mass spectrometry into the clinical laboratory.
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Comparison of phenyl-type columns in the development of a fast liquid chromatographic system for eighteen opiates commonly found in forensic toxicology. J Chromatogr A ; —9. El Mahjoub A, Staub C. Simultaneous determination of in total 17 opium alkaloids and opioids in blood and urine by fast liquid chromatography-diode-array detection-fluorescence detection, after solid-phase extraction.

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Use of high-performance liquid chromatography with diode-array detection after a primary drug screening in patients admitted to the emergency department. LC-MS analysis of serotonergic drugs. J Anal Toxicol ; —5. Liquid chromatography-mass spectrometry in forensic toxicology [review]. Mass Spectrom Rev ; — Simultaneous screening and quantitation of 18 antihistamine drugs in blood by liquid chromatography ionspray tandem mass spectrometry.

Screening, confirmation and quantification of diuretics in urine for doping control analysis by high-performance liquid chromatography—atmospheric pressure ionisation tandem mass spectrometry. Screening for 18 diuretics and probenecid in doping analysis by liquid chromatography-tandem mass spectrometry. Biomed Chromatogr ; — Marquet P. Progress of LC-MS in clinical and forensic toxicology [review]. Is LC-MS suitable for a comprehensive screening of drugs and poisons in clinical toxicology? Screening, library-assisted identification and validated quantification of oral antidiabetics of the sulfonylureatype in plasma by atmospheric pressure chemical ionization liquid chromatography-mass spectrometry APCI-LC-MS.

LC-MS-MS analysis of the neuroleptics clozapine, flupentixol, haloperidol, penfluridol, thioridazine, and zuclopenthixol in hair obtained from psychiatric patients. Simultaneous screening for drugs in blood by liquid chromatography-ion spray tandem mass spectrometry with multiple-reaction monitoring.

Evaluation of electrospray ionisation liquid chromatography-tandem mass spectrometry for rational determination of a number of neuroleptics and their major metabolites in human body fluids and tissues. Comparison of a preliminary procedure for the general unknown screening of drugs and toxic compounds using a quadrupole-linear ion-trap mass spectrometer with a liquid chromatography-mass spectrometry reference technique. A general unknown screening procedure for drugs and toxic compounds in serum using liquid chromatography-electrospray-single quadrupole mass spectrometry. Fully-automated systematic toxicological analysis of drugs, poisons, and metabolites in whole blood, urine, and plasma by gas chromatography-full-scan mass spectrometry.

Systematic analysis of acid, neutral and basic drugs in horse plasma by combination of solid-phase extraction, non-aqueous partitioning and gas chromatography-mass spectrometry. Methods for GC-MS. Weinheim: Wiley-VCH, — Drummer OH, Gerostamoulos J.

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Postmortem drug analysis: analytical and toxicological aspects. Kintz P, Samyn N. Use of alternative specimens drugs of abuse in saliva and doping agents in hair [review]. Kintz P. Substance abuse in sports: detection of doping agents in hair by mass spectrometry.

Fully automated determination of amphetamines and synthetic designer drugs in hair samples using headspace solid-phase microextraction and gas chromatography-mass spectrometry. J Chromatogr Sci ; — The simultaneous determination of codeine, morphine, hydrocodone, hydromorphone, 6-acetylmorphine, and oxycodone in hair and oral fluid. Simultaneous, quantitative determination of opiates, amphetamines, cocaine and benzoylecgonine in oral fluid by liquid chromatography quadrupole-time-of-flight mass spectrometry.

Development of a rapid and sensitive method for the quantitation of amphetamines in human plasma and oral fluid by LC-MS-MS. Determination of drugs of abuse in meconium [review]. Estimates of illicit drug use during pregnancy by maternal interview, hair analysis, and meconium analysis. J Pediatr ; —8. Detection of drugs of abuse in nails. J Anal Toxicol ; —8. Evaluation of automated single mass spectrometry to tandem mass spectrometry function switching for comprehensive drug profiling analysis using a quadrupole time-of-flight mass spectrometer.

Rapid Commun Mass Spectrom ; — Validated electrospray LC-MS assay for determination of the mushroom toxins alpha- and beta-amanitin in urine after immunoaffinity extraction. Rapid Commun Mass Spectrom ; —6. Maurer HH, Kraemer T. Amphetamine-derived Designer drugs: metabolism and screening procedures [review]. J Lab Med ; — Quantitative analysis of tropane alkaloids in biological materials by gas chromatography-mass spectrometry.

Anal Chem ; —8. Suitability testing of commercial solidphase extraction sorbents for sample clean-up in systematic toxicological analysis using liquid chromatography- tandem mass spectrometry. Annesley TM. Ion suppression in mass spectrometry. Clin Chem ; —4. J Am Soc Mass Spectrom ; —4. Ion suppression effects in liquid chromatography-electrospray-ionisation transport-region collision induced dissociation mass spectrometry with different serum extraction methods for systematic toxicological analysis with mass spectra libraries.

Rapid Commun Mass Spectrom ; —5. Mechanistic investigation of ionization suppression in electrospray ionization. J Am Soc Mass Spectrom ; — Acyl glucuronides revisited: is the glucuronidation process a toxification as well as a detoxification mechanism? Drug Metab Rev ; — Weinheim: VCH Publishers, — Improved solid-phase extraction method for systematic toxicological analysis in biological fluids.

Applicability of various brands of mixed-phase extraction columns for opiate extraction from blood and serum.

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J Chromatogr B Biomed Appl ; — Sporkert F, Pragst F. Optimum methamphetamine profiling with sample preparation by solid-phase microextraction. J Forensic Sci ; —7. Fully automated determination of cannabinoids in hair samples using headspace solid-phase microextraction and gas chromatography-mass spectrometry.

Automated headspace solid-phase microextraction and in-matrix derivatization for the determination of amphetamine-related drugs in human urine by gas chromatography-mass spectrometry.

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Solid-phase microextraction of human plasma samples for determination of sufentanil by gas chromatography-mass spectrometry. Casari C, Andrews AR. Application of solvent microextraction to the analysis of amphetamines and phencyclidine in urine. New method of derivatization and headspace solid-phase microextraction for gas chromatographic-mass spectrometric analysis of amphetamines in hair.

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Highly sensitive analysis of methamphetamine and amphetamine in human whole blood using headspace solid-phase microextraction and gas chromatography-mass spectrometry. J Mass Spectrom ; —9. Detection of 4-hydroxycoumarin anticoagulants and their metabolites in urine as part of a systematic toxicological analysis procedure for acidic drugs and poisons by gas chromatography-mass spectrometry after extractive methylation.

J Chromatogr B ; — Screening procedure for detection of dihydropyridine calcium channel blocker metabolites in urine as part of a systematic toxicological analysis procedure for acidics by gas chromatography-mass spectrometry GC-MS after extractive methylation. J Anal Toxicol ; —9.

Derivatization procedures for gas chromatographic-mass spectrometric determination of xenobiotics in biological samples, with special attention to drugs of abuse and doping agents [review]. Simultaneous screening and detection of drugs in small blood samples and bloodstains. Forensic Sci Int ; —6. Int J Legal Med ; — Staerk U, Kulpmann WR.

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Related Articles. Figure 3 shows the result of the PCA model of urine from the treatment and control groups. The flow rate was 0. Looks like you are currently in Finland but have requested a page in the United States site. The increase in cholic acid, 4-pyridoxic acid, kynurenine, and indoxyl sulfate and the decrease in UA and GA suggested that exposure to a mixture of OP pesticides induced oxidative stress and affected the antioxidant system. Given the uncertainty of the health risks of exposure to multiple chemicals, research on chemical mixtures is and will remain a key health issue. Gemini, and earlier Apollo lines in the Browse Gallery!

High-temperature solid-phase microextraction procedure for the detection of drugs by gas chromatography-mass spectrometry. Mass spectral library of drugs, poisons, pesticides, pollutants and their metabolites, 3rd ed. Mass spectral library of drugs, poisons, pesticides, pollutants and their metabolites, 4th ed. Mass spectral and GC data of drugs, poisons, pesticides, pollutants and their metabolites, part 5, 2nd ed.

Weinheim:Wiley-VCH, , in preparation. Mass spectral database. Registry of mass spectral data, 7th ed. Detection time of drugs of abuse in urine. Acta Clin Belg ; — Validation of qualitative chromatographic methods: strategy in antidoping control laboratories. Chemistry, pharmacology, toxicology, and hepatic metabolism of designer drugs of the amphetamine ecstasy , piperazine, and pyrrolidinophenone types, a synopsis. In: Rasanen I, editor.

Helsinki, Dtsch Med Wochenschr ; — Piperazine-like compounds: a new group of designer drugs-of-abuse on the European market. Neue synthetische Drogen: Piperazin-, Procyclidin- und alpha-Aminopropiophenonderivate. Toxichem Krimtech ; — Drug Metab Dispos ; — Xenobiotica ; — The action of amfepramone on neurochemical and behavioral markers in rats.

Proc Western Pharmacol Soc ; —7. Methcathinone: a new and potent amphetamine-like agent. Pharmacol Biochem Behav ; — Kalix P, Glennon RA. Further evidence for an amphetamine-like mechanism of action of the alkaloid cathinone. Biochem Pharmacol ; —9.